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After you complete the U-Bahn quest and rescue Dr. Gruselheim, you have several options of what to do with him. One option is to have him work for you, in which case it unlocks a sector operation to create new Kompositium, albeit at a slow rate (about 2 days to make one). The alternative options are to send Gruselheim to prison, and if you have been exposed to the relevant quests it is possible send him to the Diesel clinic or to help with the Red Rabies outbreak.
Also, I don't think it's so much "random." There is 1 easily accessible Kompositum in the lab and then another 2 if you have high enough stats to pass a test. The second time, you probably didn't have the requisite skills to get the extra 2.
Thanks for clearing that up for me - I did indeed have him work for me, acting as the new head of the sanitatarium to work on curing red rabies (even though it was already cured oddly, but I figured it needed a new leader, and us mercs weren't going to do it for sure). I don't see any way to create it now. By having him work for you what did you mean exactly? Is there some other outcome I should have chosen?
Edit: As in what exact sector.
If you send him to the Sanitarium (for Red Rabies) for to the Diesel Clinic, then you will get the good ending (for Red Rabies or Diesel) regardless of whether or not you successfully completed those quests.
It is a completely different option to have him work for you to create new weapons/materials. That opens up a different sector operation to craft more Kompositum.
Unfortunately, if you sent him to the Sanitarium, then you can't craft more Kompositum.
It is a Wisdom and Mechanical test in sector G12U (underground)